Well i gave this a go on Saturday as it was bloody hot and i really needed to use the Air Con (plus a simple 2-5km drive the car was overheating).
Did as directed, but there was no hiss noise at all, but i kept filling the coolant up till full, making sure that the reservoir hose was clamped to not overfill.
Let the car run for a good 10-15 minutes before i drove it.
Took it for a 3 hour solid drive and it didn't overheat at all, it sat roughly 1-2mm over the 1/4 line, which was great.
Checked coolant level later on from reservoir and it was still all fine, just like before i did it.